氢氧化钾相信大家都不陌生了吧,那么它的质量指标是什么呢?接下来跟随小编一起简单了解一下吧。
It is believed that everyone is familiar with potassium hydroxide. What is its quality index? Let's follow Xiao Bian to have a brief understanding.
1、水不溶物:5%氢氧化钾试样水溶液应无色透明。
1. Water insoluble matter: 5% potassium hydroxide sample aqueous solution shall be colorless and transparent.
2、铅:取试样1g溶于5ml水和11ml稀盐酸试液的混合液中,冷却。以此作为试样液按GT-18方法测定。对照液中的铅离子量取10μg。
2. Lead: Dissolve 1g of sample in 5ml water and 11ml dilute hydrochloric acid test solution, and cool it. Take this as the sample solution and determine according to GT-18 method. The amount of lead ion in the control solution is 10 μ g。
3、碳酸盐:在含量分析中介于酚酞和甲基橙终点之间所耗的每mL1mol/L硫酸,相当于碳酸钾138、2mg。
3. Carbonate: every mL1mol/L of sulfuric acid consumed between the end points of phenolphthalein and methyl orange in content analysis is equivalent to 138 and 2mg of potassium carbonate.
4、重金属:取试样670mg,溶于5ml水和5ml稀盐酸试液(TS-117)的混合液中。加热沸,冷却,用水稀释25ml,后过滤。以此作为试样液,按GT-16方法测定。用含20μg铅离子的对照液(溶液A)。
4. Heavy metal: take 670mg sample and dissolve it in 5ml water and 5ml dilute hydrochloric acid test solution (TS-117). Heat to boiling, cool, dilute with water to 25ml, and filter. Take this as the sample solution, and determine according to GT-16 method. 20 for use μ G Reference solution of lead ion (solution A).
5、汞:按CT-22方法测定。标准液和试样液按如下方法制备。
5. Mercury: determined according to CT-22 method. The standard solution and sample solution shall be prepared as follows.
(1)标准液的制备:按GT-22制各贮液和稀释液,使所得溶液每ml中含汞1μg。取该溶液1ml,放入-50ml烧杯,加水20ml.1:4稀硫酸溶液1ml和4%高锰酸钾溶液1ml。用表面皿盖住烧杯,煮沸数秒钟后冷却,备用。
(1) Preparation of standard solution: prepare each storage solution and diluent according to GT-22, so that each ml of the obtained solution contains 1 mercury μ g。 Take 1ml of the solution, put it into a - 50ml beaker, and add 20ml of water 1: 4 Dilute sulfuric acid solution 1ml and 4% potassium permanganate solution 1ml. Cover the beaker with a watch glass, boil it for a few seconds, and then cool it for standby.
(2)试样液的制备:取试样10.0g放入-100ml烧杯,加水15ml使之溶解,加酚酞试液(TS-167)2滴,在不断搅拌下用1:1稀盐酸溶液缓慢中和。加1:稀硫酸溶液1ml和4%高锰酸钾溶液1ml,用表面皿盖住烧杯,煮沸数秒钟后冷却,备用。
(2) Preparation of sample solution: put 10.0g of sample into a 100ml beaker, add 15ml of water to dissolve it, add 2 drops of phenolphthalein test solution (TS-167), and slowly neutralize it with 1:1 dilute hydrochloric acid solution under constant stirring. Add 1ml of 1: dilute sulfuric acid solution and 1ml of 4% potassium permanganate solution, cover the beaker with a watch glass, boil for a few seconds, and then cool down for standby.
The above quality indicators of potassium hydroxide will be briefly introduced here. If you have anything unclear, please contact us directly http://www.jinhao360.com Right.